مشخصات پژوهش

صفحه نخست /A molybdenum(VI) Schiff base ...
عنوان A molybdenum(VI) Schiff base complex immobilized on functionalized Fe3O4 nanoparticles as a recoverable nanocatalyst for synthesis of 2-amino-4Hbenzo[ h]chromenes
نوع پژوهش مقاله چاپ شده
کلیدواژه‌ها Dioxomolybdenum(VI) complex, Three-component, Fe3O4
چکیده A dioxomolybdenum(VI) complex of a Schiff base, immobilized on the surface of modified Fe3O4 with a silica coating, has been synthesized and characterized by spectroscopic and microscopic techniques including FTIR, TGA, ICP, SEM, EDX, VSM, and XRD analyses. The catalytic performance of this material has been evaluated for the preparation of 2-amino-4Hbenzo[ h]chromenes via the one-pot, three-component reaction of aldehydes, malononitrile, and 1-naphthol under solventfree conditions. The benefits of this protocol are short reaction time, simple workup procedure, and high yields of products. Also, the synthesized nanocatalyst could be separated easily from the reaction mixture using an external magnet and reused for four consecutive times with only minor degradation of its catalytic performance.
پژوهشگران الهام مرادی خرمنانی (نفر دوم)، نیاز منادی (نفر اول)