عنوان
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Intercalation of supramolecule into LDH for solid-phase extraction of NSAIDs in water and urine sample
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نوع پژوهش
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مقاله ارائه شده
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کلیدواژهها
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Layered double hydroxide, supramolecular chemistry, Real samples, Calix[4]arene
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چکیده
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The present research aims to prepare a new sorbent based on an acidic calixarene (A2CA) intercalated into a Mg/Al layered double hydroxide (LDH) to achieve the new sorbent (A2CA@LDH) (Scheme) which was confirmed by utilizing techniques [1]. The prepared sorbent's ability to extract specific nonsteroidal anti-inflammatory drugs (NSAIDs), from water and real urine samples was examined using the pack column strategy. Plackett-Burman and Box-Behnken designs, two components of the response surface methodology (RSM), were utilized to fine-tune and optimize the parameters controlling the extraction and desorption process by using an HPLC-UV. The results demonstrated that this new sorbent and current method may be helpful for accurately, easily, and affordably identifying NSAIDs in actual samples [2].
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پژوهشگران
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میلاد غنی (نفر سوم)، رحمان حسین زاده (نفر دوم)، Navid Sahebjamnia (نفر اول)
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