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Title Green synthesis of tetrahydrobenzo[b]pyrans, pyrano[2,3-c]pyrazoles and spiro[indoline-3,4′-pyrano[2,3-c]pyrazoles catalyzed by nano-structured diphosphate in water
Type JournalPaper
Keywords tetrahydrobenzo[b]pyrans, pyrano[2,3-c]pyrazoles, spiro[indoline-3,4′-pyrano[2,3-c]pyrazoles, nano-structured diphosphate, water
Abstract A green and recoverable nano-structured diphosphate (Na2CaP2O7) was synthesized and fully characterized using FT-IR spectra, X-ray diffraction patterns (XRD), scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDX) analysis. The nanostructured catalyst has been successfully used as reusable nanostructured catalyst for green, simple and efficient synthesis of tetrahydrobenzo[b]pyrans, pyrano[2,3-c]pyrazoles and spiro[indoline-3,4′-pyrano[2,3-c]pyrazoles in aqueous media. The catalyst shows environmentally benign character, which can be easily prepared, stored, and recovered several times without obvious significant loss of catalytic activity.
Researchers Hossien Ali Akhlaghi (Fifth Researcher), Amir Khojastehnezhad (Fourth Researcher), Reza Tayebee (Third Researcher), Negar Nasiri (Second Researcher), Behrooz Maleki (First Researcher)